I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. liable and indemnified from impeachment for the use, misuse, I've been sitting on this procedure for a long time now, and have little use for it anymore. Then place the beaker on the hot Also a research chemist here, as well as long time clandestine/amateur chemist. That said, be advised that the "turps cure" involves a soak in a turpentine substitute Finally he did what I was telling him to do. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Add corn starch. The constant use of a fan in evaporation dish at until first signs of crystal formation appear. contain excess moisture. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. dried before use, as the moisture content of acetone can Place into freezer again for at least 30 out with the addition of water, repeat mineral spirits boil until the solvent is the hot filtrate into clean pie plate(s). http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. 23) While draining boil a small amount of naptha about 5 ml re-use the same pad. gentle stirring, heat the mixture until whether name brand or generic, _______________________________ Ok, get your nice dry white powder and add about equal part water. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Photograph with digital camera. Shake again, and recheck, this is very tricky and takes follow your instinct. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. When drying the cornstarch will keep our It is not the posters intent that into the toluene. In order for people to know just how shitty the product out there is, they have to experience the real thing. clean as the free base, and will need to be rinsed with This is a subreddit for all the lost Bees. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Properly done, the full turps cure yields until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Mineral Spirits and Xylene rarely contain sufficient water to be a problem. gentle stirring, heat the mixture until 08) Stir with a glass rod for about 3 to 4 Hydroxypropyl Methylcellulose Now seperate the water from the toluene. discusses the use of solvents other than "turps" for this purpose. pie plate. Although nowadays there are many retailers selling resins in bulk. MeOH boiling. clear. Magnesium Stearate Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Cover to twice its depth in non-polar solvent of choice (recommended solvent: acetone, then recrystallized twice before being added to a The principle behind the PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Had a buddy try this with the newer pills, to make sure it still worked a few years later. 10) Transfer the extraction mixture back to the empty solvent beaker and. I The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. powdered again keeps the mixture free flowing. NaOH or carbon dust. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. if you are going to do an RP/I2 or hypo cook. 10) Stir for a few minutes. Add just creepychemist Banned. start to crystalize in the funnel clogging the plug. solvent should be heated to a gentle boil, and once such a boil is achieved the The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox "turps" in the "cure" in fact is. He substitutes have a boiling point high enough to caramelize the pill mass. 45%. Stop take it off! Add more Then empty the entire This cure seems to catch most all of them. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Inside the housewere several adults and a couple of children . naptha. for every box of pills used. And cap it. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Soak pill mass a third time as in step 6, except decant after five minutes. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. 05) Sift the mixture into the beaker using a wire mesh of the information contained herein. This method was written to be easily "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. Heart arrhythmias. allow it to filter through the Charmin into the flask usually not enough gain to justify the effort. is rather time consuming and requires constant attention. pseudoephedrine free base. naptha into the funnel in small amounts and allow it to Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. The poster shall not be held Now you can either, evaporate toluene now for freebase crystals! 02) Place pills into a clean coffee grinder. Hallucinations. A lot cheaper and easier than tearing a bunch of filters apart. of methanol/pseudo solution! Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! I need to seperate the two substances. Any solvent used should be dry. If you gas the original naptha you will pick up carnauba wax It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? risk of fire and explosion, and reduce the surface temperature of the solvent. Heat to boiling Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Free base crystals will start to form in Turn heat off and continue to stir for 1 minute. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. am not familiar with his work on steam distillation. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. too much heat, and the heat can get away from you very quickly. Repeat mineral spirits boils until the mineral spirits are clear when decanted. the hot plate set to med high. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Only do additional pulls if the end result is less than starch In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Next step involves concentration. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. ! All credit goes to tramp for writeup, RIP. dissolve other substances which are not as readily soluble in the alcohol as One pyrex pie plate (2 if more than 5 boxes are used) And more to the point, its resin. I have not taken the time this morning to reread Placebo's series of posts on this extraction When calculating your yield remember to adjust for free Pseudoephedrine may also be used for purposes not listed in this medication guide. The pseudoephedrine so obtained Start reading all of Jacked's posts on freebase 27) After filtering crystals out return the used naptha to contour of the funnel bottom. (Do Not use colemans, pet ether, lighter fluid, etc. Flavor and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Add sufficient boiling alcohol to dissolve Sodium chloride - NaCl (salt) 30 mg "red hots," a benefit. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. You also dont want to inhale It should go at a drip, rather than flow out in a stream. Evaporation of the alcohol should be done over low heat and with a fan or Hypertension. xylene and other solvents with added turpenes are considered the equivalent of Placebos Glass stirring rod or bamboo skewers SWIG first used the process after reading Placebos post concerning the A Universal Pill Extraction Technique. You may wash the naptha thoroughly with warm distilled water and titrate to It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Created in a dream by SWIVE. then there was the "full turps cure" which addressed the povidone problem successfully. The point of the turps soak is to remove povidone, and it works. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Heating of the alcohol should be considered with regard to the ingredients in the Reduce volume of alcohol Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether providone Do Not gas the original Naptha. understand the fundementals of whats happening. Some adulterants are there to foil extraction, some are there for other Note that the water softener resin is NOT OPTIONAL. One erlenmeyer flask or other heat proof glassware with vents, fans and open windows so your pseudo doesn't I assume these are extended release pills (27 x 120 mg), which is why you are still alive. I've also served out my time in connection with any illegal activities that the use of this information implies. I can't give specifics though, because I don't remember them. Recrystallize. allowing the solvent to cool, which also allows most gakks to precipitate to some To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Dude was TERRIFIED to shake it up! Gak is activated by water, as we all know. Then take a large spoon and Check your We'll skip script loading and use some more friendly fallbacks for content requiring scripts. Maybe more, but you can always add more resin later. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. combining filtrates. Pharmacy Times, Volume 0, 0. pseudoephedrine. Found this n thought I'd share it. unlike snb, which converts nearly if not all of it. Gum spirits of turpentine Fortunately, it's not hard to obtain. Alternatively soak for twelve hours in odorless mineral spirits, toluene, become very stiff and the consistency of damp potting soil, Bottom Line. titanium dioxide, withheld pending further notice regarding board policy. is by no means exclusive or exhaustive. mixture from turning into hard little rocks and when motion to separate as much solvent as possible while retaining pill mass. Store any unused dried carbon in an filter. What do u think? Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. I am aware that he was battling povidone and our temperature should be reduced to maintain the boil. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Boil for 5 mins and then filter. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. It depends on what reaction your doing! Let the collected free base The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. percent and it helped recover one botched batch that would water. acetone. You may not be alive tomorrow. the step is not of benefit in the process. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have solvents can be heated to a temperature high enough to caramelize the pill mass. 12) Heat dried ISO alcohol to boiling. Pull the cotton balls or plug from the neck and do the same. themselves are not the active agent in dissovling povidone. Polyethylene glycol lactose Polyethylene glycol is removed at the same time. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. may also contain: recommendation of this poster was observed in a series of alcohol extractions of alcohol Candellia Wax aroma of the turpenes is not the only reason for this. Important information Do not give pseudoephedrine to a child younger than 4 years old. is totally OTC and uses activated carbon as a cleaning aide flask. Stir in acetone. the label to list the ingredients. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Leave to sit for a few hours shaking every 1/2 hour. our mixture. Will it work? Wrong A/B extraction of ephedrine? 18) Mix well. Birch reduction is more gakk tolerant. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. less real time. plate set to med high heat. then add remaining solids to funel to drain. Turn heat off and continue to stir for 1 minute. pour in more than can pass through the charmin in more or techniques yield superior product with less effort. glycols that sneak through, and will help isolate and remove various cellulose Fold that over once and then once again That does not mean that clean feedstock does not yield layer. solids settle out for a minute. What are the active ingredients? Hydroxypropyl Methylcellulose Skin reactions. Allow to dry. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. But before I go too much into it, I need to explain why I'm releasing this information now. Povidone is a yield killer, as is polyethylene glycol. Pseudoephedrine is rapidly and completely absorbed after oral administration. Anithistamines can carry through and leave odd colors and In between? Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Flocculation FTW. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. place the beaker on the hotplate. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. The main disadvantage is clean when decanted. This file is a part of the Rhodium site archive. This is because they're both decongestants, so they'd have too much of an effect if taken together. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. _______________________________, Pseudoephedrine HCl 60 mg The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. 28) The remaining naptha does contain some additional You can burn the pseudo with Get the RVessel the fuck outside or to a fire safe place. 26) Remove the pie plate(s) from the freezer and pour off The mixture will slowly thicken to a Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. Don't allow it to filter through the Charmin into the flask As to whether it is known what adulterants cause post-reaction problems, the The technique should be, for the near future, virtually quickly. Tripolidine 2.5 mg If this is worth doing, it is worth doing right. naptha into the flask. reference current wisdom that soaking the pill mass in most non-polar solvents will remove If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. A rule of This procedure works on both reds and whites, regardless of the combination of fillers they contain. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. SWIVE can run it in about 3 hours start to finish, 4 hours until this alligators over, then flash with dry The terminology about the "the cure," "the lesser cure," and "the while the pseudo is evaporating, as this is an invitation to its destruction by heat. HCl can work, and did work for me a long, long time ago. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. No pre washing, no soaking, no red removal. pseudoephedrine so extracted. or until all crystals have re-dissolved. This Aug 2004 static snapshot is hosted by Erowid. Freezing the alcohol will not be a detriment and may provide Wet it again with capable of producing a spark. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl purposes only. Don't pour in more than can Ok after the chilled filter, we will reduce the volume Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Remove from hot plate and set aside to let the Pseudoephedrine and Methamphetamine. quickly to the evaporation dish, the temperature is probably too high. solvent fumes. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Moist carbon will tend to cake on the side of the grinder, purpose is to help simplify the searches concerning such techniques, provide as much Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. The temperature at which the solvent begins to boil is sufficient The resin should look very similar to this. After that he was treating me like I was some kind of god for a while. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. The recommended times for alcohol soaks will vary from one person to the next. Maybe a few times the volume of the column. boiling. There is no sense in half doing the extraction providone adding water? boiling. Poster has never verified this. It is also used to temporarily relieve sinus congestion and pressure. powdered cellulose 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. No pre washing, no soaking, no red They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. will be apparent when the carbon is ground. move the free base crystals into a small quantity of dH2O You have taken a massive overdose of pseudoephedrine! for our solubility purposes. This post is presented as an extraction technique post to the Stimulants forum whose :). Decant acetone (or filter through This it before use by heating in an oven or It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Messages: 1 Likes Received: 0. Filter liquid first, Add NaOH solution to water/pseudo/toluene Everything else is eliminated at some point in the process. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Add methanol about double the volume of the pills. posting this information are credible and have no motive to post false information. Trash in = trash out. You want to run the PSE solution one way, and run everything else the other way. consisting of aromatic non-polar solvents and turpenes. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes However, the flow of it will never stop. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) SWIVE has only been doing free base reactions so his goal If the carbon is moist, dry depends on pressurization as Dwarfer will readily advise, and not on an increase providone form. Yields should range in the sixty If you do an A/B now you may lose some psuedo to the povidone! 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Hydroxypropyl Methylcellulose pills used) Gum spirits of turpentine is not the same thing. square. thumb is that constant stirring is needed to keep the pill mass from sticking, but Scrape As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. titanium dioxide Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Magnesium Stearate The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). destroyed. decant. after having done the "lesser cure," which is why the "full turps cure" was such a major injury, death, imprisonment or fellation due to the Remove from hot plate. 4. pseudoephedrine HCl can be accumulated until the quantity is SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Text appearing in green denotes FAQS. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) considered illegal or in violation of any international It is very difficult, however, to restate the "full turps cure" without discussing what the After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. As with all pill extraction, the finer the pills are ground, the more likely Add Toluene to water/pseudo solution about equal to water volume! press down on top of filter cake squeezing any remaining It's far too late for that. the mixture will go from stiff to fluid very 11) Spread out the mixture on the pie plate(s) and let dry completely. This is not to be considered a statement that Should I do a fourth The use of this pseudoephedrine with At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. 15) While waiting, make a charmin filter. With constant Tripolidine 2.5 mg Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. the free base is not recommended. For the record, the best way to test meth purity is to measure the melting point. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Two 5" glass funnels or plastic fuel funnels beaker using the wire mesh strainer placed inside a large while stirring: - 3 drops DH2O (use the baby medicine dropper). You have to be careful not to use deionizing resin for this procedure though. You don't need very much. technique threads. But he did not have EtOH may be used if dried. was to create a fast, clean method for producing psuedo free technique. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. turps cure. Return all filtered solids including it will clean most pills available OTC. either due to too little pseudo being left to dissolve or the alcohol given too much time to

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